From environmental analysis to pharmaceutical water: A comprehensive overview of the TOC Applications
TOC
Analyzers are used to determine the
Total Carbon as well as the Total Inorganic carbon present in a sample. The technique
used by the analyzers is used to determine the proportion of both non-volatile
as well as volatile compounds. In procedures such as wastewater management, TOC
determination measures the sample for low or high TOC content. TOC
analyzer are used in a wide range of industries including the
management of effluent, ultrapure water, management of pharmaceutical water,
drug manufacturing process, environmental investigations of soils and river
water, and the evaluation of cleaning efficiency.
How do TOC works?
For TOC analyzers, that
account for the total as well as the inorganic carbon, there is a two-stage
analysis technique, called TC-IC. This process is used to measure the total
amount of inorganic carbon evolved from an acidified aliquot. On the other
hand, there is another technique known as the TIC-NPOC analysis method.
Nevertheless, whether it is by the NPOC method or the TC-IC method, the
analysis of the Total Organic Carbon can be broken into three main stages.
#1 Acidification
In the acidification
process, the removal of PC and IC gases occurs. Here an acid is added and the
inert gas sparing transforms all the bicarbonates and carbonates ions into
carbon dioxide. After that, the IC product is then vented along with any sparse
purge able organic carbon present in the mixture.
#2 Oxidation
In the TOC analysis
process, step-by-step oxidation occurs through a series of processes in the
chronological order of their high-temperature combustion. The processes in
their order can be listed as:
- High-temperature
catalytic oxidation or HTCO
- Photo Oxidation
- Thermo-chemical
oxidation
- Photochemical
oxidation
- Electrolytic
oxidation
#3 Detection and
Quantification
In the TOC analysis
process, accurate detection and quantification are the most critical components.
Typically there are two usual detection methods used in the new-age TOC
analyzers. The typical detection methods include conductivity
techniques and non-dispersive infrared or NDIR methods. There are essentially
two types of analyzers. The former one uses combustion for analysis purposes,
whereas the other one uses chemical oxidation. Generally, in the second
process, the water purity is tested to detect the presence of organic carbon or
the unwanted pathogens present in the sample.
Just like the TOC
analyzer, there are other reliable methods as well like the N/C technique
reliable which is versatile and easy to use. It is a brilliant series that
offers insightful user guidance with precise analytical work.
The bottom line
Elemental chemistry has
witnessed some unprecedented dynamism in the past few decades. The purity of a
sample or substance is of critical value in the world of manufacturing and
manufacturers all across the globe are using oxidation techniques including TOC
analyzers to understand the purity of water. Undoubtedly, TOC analyzers
are of paramount significance, but accuracy is everything when you are working
with elemental analysis. Always opt for the professionals when you are seeking
TOC analysis, and the results will always come up to be reliable.
Frequently Asked Questions:
·
What is ICP-OES?
ICP optical emission spectrophotometers (ICP-OES) began to
be widely used, and is now one of the most versatile methods of inorganic
analysis. Its features are often compared to atomic absorption
spectrophotometers.
·
What is ICP-OES Principle?
ICP, an abbreviation for Inductively Coupled Plasma, is one
method of optical emission spectrometry. When plasma energy is given to an analysis
sample from outside, the component elements (atoms) are excited. When the
excited atoms return to low energy position, emission rays (spectrum rays) are
released and the emission rays that correspond to the photon wavelength are
measured.
·
How does ICP-OES work?
ICP-OES works by first using a peristaltic pump to conduct
the sample through a nebulizer and into a spray chamber. After being converted into
an aerosol, it is fed into an argon plasma via the use of a cooled induction
coil, which induces an alternating magnetic field and sends accelerated
electrons into a circular trajectory.
·
What is ICP-OES used for?
The technique of ICP-OES is employed in a wide variety of
industries for a number of different applications. For example, it is commonly
used in the oil extraction and refinery sectors to analyses oil samples for
impurities in the commodity.
·
What are Common problems with
ICP-OES?
Common problems with ICP-OES are:
1.
Poor precision
2.
Sample drift
3.
Non-ideal detection
4.
Inaccurate identification
·
What is the difference between
ICP-OES vs ICP-MS?
ICP-OES is often compared to ICP-MS. ICP-MS operates using many of the same principles as ICP-OES, except that the detection of elements from the aerosolized and ionized sample occurs via mass spectral analysis rather than being based on photon emission.
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